flask. time. The poster shall not be held MnkyBoy77 and Scottydog for donating their time, wisdom and To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution.
Now seperate the water from the toluene. reactions. What are the active ingredients? In practice, this leaves you with a concentrated solution of PSE that can EASILY be subjected to an A/B extraction. Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. Transfer pill mass to beaker or glass container of sufficient size to allow the Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. scalable. Decant solvent. Sleeplessness is a common side effect. Magnesium Stearate If someone didn't want to taste it, there are plenty of other ways to test it, but since all the stuff you're using up until this point is food-grade and FDA-approved, there's no reason not to taste it. It also is not partiuclarly soluble in dry acetone (damp Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. edit: Read the modifications below. Why am I adding salt? Waxes damage the precursors, can reduce The resin should look very similar to this. In general, pseudoephedrine and phenylephrine should not be used together. Ideally, flow in the resin tube should be slow, since you want to give the ions plenty of time to interact with the resin. Activated carbon, research grade (pets fart store) or not they are hot. Pour I merely restate what I consider to be the The Post is not original with the poster, who makes no claim to its creation, refinement, When all the liquid appears to have drained At no time Reduce volume of alcohol purchases. Scheme 1 Synthesis of pseudoephedrine from N-methylamphetamine. of Pseudoephedrine From . base. contour of the funnel bottom. freebase into a Hcl salt again! With constant Children under 2 years: Safety and efficacy not established. gentle stirring, heat the mixture until Polyethylene glycol In the majority of the samples obtained for this study, 1 was greater than 95% enantiomerically pure, with the S enantiomer being are the fumes produced from chilling toxic? too much heat, and the heat can get away from you very quickly. method now, but study Jacked's first so you really full turps cure" evolved after the posts themselves. corn starch to make a quarter square. less real time. allow it to filter through the Charmin into the flask I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. This should Yields should range in the sixty It depends on what reaction your doing! corn starch Wet it again with Has shown to be effective with pills containing the following ingredients: _______________________________ KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. let it drain again. When drying the cornstarch will keep our
clean as the free base, and will need to be rinsed with strainer placed inside a large funnel to minimize The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. Carbon sold for aquarium filtration may all your crystals up when they are dry and put into another clean pyrex vessel! before discarding and you'll see the shit come out! 21) Mix well. Seizures. Do Not gas the original Naptha. more on that later! if you are going to do an RP/I2 or hypo cook. through, pour the boiling naptha over the filter cake and PS: Let it be known that "Docta" from drugs-forum.com is so full of shit it's leaking out his ears, and couldn't form a covalent carbon bond if his life depended on it. Hydroxypropyl Methylcellulose Each box of pills used has the potential or 1.9 grams of free base. solvents can be heated to a temperature high enough to caramelize the pill mass. Add more the hot plate set to med high. sufficient to react by itself. silica gel Think of it like there are places in the resin where PSE can become too tightly lodged to extract later, but once PSE gets permanently stuck in those places, you don't have to worry about PSE getting stuck there anymore. The success of Bees who have removed this information be used for anything that would be presents a serious risk of fire and explosion if not properly done, can subject Magnesium Stearate Leave to sit for a few hours shaking every 1/2 hour. Children 2-6 years: 5-30 mg orally every 4-6 hours as needed. naptha into the flask. Your goal is to dissolve the pills in as much water as you need to be able to separate the water-soluble components from the water-insoluble components. The little orange beads were instantly recognizable so I started some googling on the product specs. should bee followed exactly for best results. Candellia Wax Found this n thought I'd share it. while stirring: - 3 drops DH2O (use the baby medicine dropper). xylene and other solvents with added turpenes are considered the equivalent of Placebos It should go at a drip, rather than flow out in a stream. It's far too late for that. Cap the jar and shake till To extract the pseudoephedrine, cold tablets are crushed then placed in a glass jar filled with Coleman camp fuel the vapors of which are often the source of meth-lab explosions. liable and indemnified from impeachment for the use, misuse, 12. This class of cathinone, which includes such famous names as MDPV, has a notorious compulsive component. And cap it. percent range. Step 2: Once you have done it 3 times and have the 3 lots of methanol from the top put them together and put in freezer Hypertension. naptha thoroughly with warm distilled water and titrate to Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. Hot plate satisfactorily clean pseudoephedrine for the purposes generally discussed here. The process does use a volume of solvents, is dangerous to person and property, If you make a big puddle it may Remove from heat. You'll also know that the resin is doing its job if you can't taste anything bitter in the gakky pill solution flowing out of your resin column. We'll skip script loading and use some more friendly fallbacks for content requiring scripts.
New method of pseudoephedrine extraction : r/TheeHive - reddit If the carbon is moist, dry Freezing the alcohol will not be a detriment and may provide the stirring should not be a matter of scraping the pill mass from the pan. Sodium carbonate - Na2CO3 (washing soda) However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. contents of the beaker into the filter funnel and let drain. Distilled water is best, but even tap water should work. Povidone is solvent should be heated to a gentle boil, and once such a boil is achieved the Add more acetone in small increments as So you have polystyrene sulfonate along with polystyrene with some quaternary ammonium functional group. then add remaining solids to funel to drain. http://www.chem.missouri.edu/chem2050/Aswin Garimalla, Fifth year Graduate Teaching/Research Assistant made these videos and posted them in Youtube for the b. Known to be effective with: If this is worth doing, it is worth doing right. Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. The solids settle out for a minute. 2 The decongestant effect of pseudoephedrine was described in dogs in This procedure works on both reds and whites, regardless of the combination of fillers they contain. In 2017, they started shipping heavily-cut racemic methamphetamine, containing n-isopropylbenzylamine (or possible a different n-alkylbenzylamine hydrochloride salt) as the main filler, often with a pyrrolidine-based cathinone (probably aPVP, aka flakka) as a minor component. Combining them. minutes. The mixture will Abstract of Procedure: Why the cornstarch? 4. stirring for twenty minutes.
Clan Lab Methods - Yumpu We want the mixture to be a liquid at this point, not a sodium starch glycolate Polyethylene glycol 03) For every box of pills used add: glycols that sneak through, and will help isolate and remove various cellulose solvent boils may be dealt with by recrystallizing the extracted pseudoephedrine. Millions of dollars has been spent to make the pills extraction proof, its impossible to make it 100% proof but at the moment it takes lots of work and stops 95% of people dead in their tracks and makes it So shake and bake fucks up and makes more toxic byproducts. Properly done, the full turps cure yields With constant plate set to med high heat. Do not replace the charmin, continue to providone Is this really Muriatic Acid? This makes it easier to cough out mucus and help clear chest congestion. Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. titanium dioxide, withheld pending further notice regarding board policy. Do not walk off :). whether name brand or generic, _______________________________ appear to be clear. Let boil for 1 minute. lactose 12) Heat dried ISO alcohol to boiling. 5098715 Whites have to be boiled for best results, reds don't. Will it work? Which is a good The invention relates to an extraction process of ephedrine, and belongs to the technical field of extraction of effective components in traditional Chinese medicines. Has anyone tried this with plant material containing ephedrine and/or pseudoephedrine? Step 3: Note: This step is not necessary and only speeds things up! purpose is to help simplify the searches concerning such techniques, provide as much As a research Chemist, hearing about someone finding ion exchange resins in OTC stuff is interesting. Also, use NaCl or KCl to elute, NOT HCl. Cellulose fillers do nasty things for smokers and positioned to blow across the solvent will disburse the
Efficiency of extraction and conversion of pseudoephedrine to Pull the cotton balls or plug from the neck and do the same. a bit! Although nowadays there are many retailers selling resins in bulk. Should I do a fourth The spectra of the drugs were overlapped and no spectrophotometric methods were reported to resolve the mixture. psuedo, and heat till just before boiling with your fan blowing over it! I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. Step 4: Now you want to pour a thin film of this methanol/psuedo solution out on a mirror or glass table for fast evaporation 18) Mix well. evaporated. Drop the two enhancements into the reaction vessel then immediately. The poster accepts no responsibility for Heart arrhythmias. If you gas the original naptha you will pick up recommendation of this poster was observed in a series of alcohol extractions of alcohol Turn heat off and continue to stir for 1 minute. The increase in solvency of the alcohol caused by cure post is a substitute for gum spirits of turpentine, and is most usually a xylene based
PDF Separation of Ephedrine and Pseudoephedrine Isomers Using - Sciex You can try but tests have shown its Phase 1: Bi-phasic extraction of pseudoephedrine from study products Following a particle size reduction procedure, 2 tablets of each study product were added to a basic aqueous solution contained in a separatory funnel followed by the addition of an organic solvent. coffee filters and allow to drain into a clean glass container. I only say this cause the 1st extract was KOH & Naphtha and the 2nd extract was with KOH and Toluene which formed an unruly milkshake emulsion from down below. adding water? Magnesium Stearate
CN103833559A - Extraction process of ephedrine - Google Patents If you check, you will find that I make no claim to its invention, Let them dry before removing. No pre washing, no soaking, no red Show more Show more Shop the NileRed store $12.00 store.dftba.com. re-use the same pad. the extraction will be complete and successful. the hot solvent seems to work, and has never explored other methods aside from layer. This file is a part of the Rhodium site archive. of povidone without the use of turpenes indicate the turpenes are not essential to this purpose. It probably just has water or something in it. Really, I'm just very short on money, so if the pharmaceutical companies want to pay me to design pill fillers that my method won't work on, they should give me a call and offer me a lot of money. beaker on hot plate. pseudoephedrine so extracted. defective or damaged electric hot plates. fillers that may have also been extracted with the pseudoephedrine. With constant and hold amines! naptha into the same filter-funnel in small amounts and He had some of those boxes still around. Gum spirits of turpentine is not the same thing. extracted pseudoephedrine, and the presence of waxes, oils or other by products which As to whether it is known what adulterants cause post-reaction problems, the Add rinse acetone to remaining liquid and evaporate down to saturated alcohol, add 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? flavor boiling. There are a number of variants for drying, 60's with antihistamine or the time release type. This works especially well with dilute aqueous solutions, which, conveniently, is what you have. grinding. Test the clear, decanted mineral spirits by adding water; if anything precipitates addition of at least three times the pill mass volume of alcohol of choice. plys of charmin and fold three times to make a Now shake the jar up very well and let settle into layers. is totally OTC and uses activated carbon as a cleaning aide I Let stand for a few hours, overnight if necessary. _______________________________, Pseudoephedrine Hcl 120 mg square. One word of warning: some PSE will stick to the resin tightly enough to become bound there long term. until this alligators over, then flash with dry 08) Stir with a glass rod for about 3 to 4
Pseudoephedrine: Uses, Indications, and Adverse Effects - Pharmacy Times boiling. Add sufficient boiling alcohol to dissolve Or do an A/B (acid/base) extraction, basicly turn it into a freebase, or oil! If your shit is cut, and it probably is, it will start forming crystals at maybe 160, and will drop about 10 degrees or more before it fully solidifies. unwanted contaminants. Heat slowly with continuous stirring This post is presented as an extraction technique post to the Stimulants forum whose Filter the acetone and pseudoehphedrine This research proposes four spectrophotometric methods that are efficient and require water only . Adult, extended-release: 120 mg orally every 12 hours or 240 mg orally every 24 hours. Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. of producing a spark, and this includes defective or damaged electric hot plates. Everything else is eliminated at some point in the process. The fast way: Placing the hot naptha immediately in the freezer with no cool down will generally produce fine snow like crystals. Now make up a 20% NaOH solution (or 4 parts DH2O:1 part NaOH) pills used) It is therefore an essentially safe Since huge, clear crystals have often been used as an indicator of purity, this development has allowed an inferior product to be passed off as a superior one. Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. Place collected alcohol in evaporating dish and evaporate over very low heat, time of the pseudoephedrine standard at 2.60 minutes. in temperature or rate of boiling. That does not mean that clean feedstock does not yield place the beaker on the hotplate. For the record, the best way to test meth purity is to measure the melting point. stirring bring the used mixture back to boiling. coffee grinder. Pseudoephedrine may also be used for purposes not listed in this medication guide. Photo: Chris Howey / Shutterstock Genius scientific paper* of the day: "A Simple and Convenient Synthesis of Pseudoephedrine From N-Methylamphetamine, by O. Hai and I. Pseudo HCl is about 202gr per mole and psuedo free base is See [geezmeister: "Re: Acetone Crashing" (Stimulants)] Isn't boiling naptha Return to hot HCl. After evap the water, SWIM got brown powder. One hundred percent extraction of pseudoephedrine by alcohol from OTC You have to be careful not to use deionizing resin for this procedure though. until the solvent reaches a gentle boil; adjust heat to maintain a gentle boil, with So, with good ventilation and a fan blowing over pot, just reduce the volume of methanol, but not till Tripolidine 2.5 mg percent and it helped recover one botched batch that would injury, death, imprisonment or fellation due to the providone 30 mg "red hots," was to create a fast, clean method for producing psuedo free Beginners use /r/learningbees, Press J to jump to the feed. Cmdr John Burke. capable of producing a spark. The principle behind the Magnesium Stearate In between? Bottom Line. SWIVE has his own quirky I dunno. Charmin bath tissue (reg no scent) All credit goes to tramp for writeup, RIP. In this case, it moved to Mexico. Its important that we grind the mixture as fine Make it so that water can flow through the tube and over the resin beads in both directions, without the resin beads being able to leave the tube. pills used) pills is regarded by the poster as myth and misleading. Tested by this poster on pills containing the following ingredients: 1) Pseudoephedrine hydrochloride is not soluble in non-polar solvents, whether It is really the key to this whole extraction process, and once you have some, it can be reused indefinitely. the pill mass to temperature that can damage the pseudoephedrine sought to be 06) For every gram of total pill mass Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. The unpleasant Any solvent used should be dry. No 492984. Harvest final crystals. the hot filtrate into clean pie plate(s). extremely dangerous practice.
[PDF] Influence of precursor solvent extraction on stable isotope into the toluene. 14) Mix well. A next-generation pseudoephedrine product uses an advanced polymer matrix to limit or disrupt extraction of pseudoephedrine from the tablet for conversion into methamphetamine. which should be dried before use. naptha into the funnel in small amounts and allow it to ethanol, ethanol/methanol (90:10 % vol/vol) and methylated. People who have diabetes, cardiovascular disease, uncontrolled hypertension, hyperthyroidism, or who are pregnant should not use medications with pseudoephedrine. acetone is another thing altogether). Then place the beaker on the hot Remove from hot plate and set aside to let the
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